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Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data]
Aug 23, 2023 - Institute of Organic Chemistry - AK Mastalerz
Kirschbaum, Tobias; Rominger, Frank; Mastalerz, Michael, 2023, "Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data]", https://doi.org/10.11588/data/JE8LF7, heiDATA, V1
A benzotrisazulene was synthesized on the basis of a truxene precursor by a series of Suzuki–Miyaura reactions via the intermediate trisoxo compound. The latter occurs in two forms (syn and anti), and the syn forms porous crystals.
Etheno-bridged Azaacene Spiro Dimers [data]
May 8, 2023 - Bunz Group
Ahrens, Lukas; Rominger, Frank; Freudenberg, Jan; Bunz, Uwe H. F., 2023, "Etheno-bridged Azaacene Spiro Dimers [data]", https://doi.org/10.11588/data/L8NDRO, heiDATA, V1
We present the synthesis of two sets of spiro-connected azaacene dimers. Their geometry and electronic coupling are critically determined by a secondary linker, i.e. an etheno- and an ethano-bridge.The core fragment of the etheno-bridged dimer corresponds to a conformationally lo...
Cyclopentannulated Dihydrotetraazapentacenes [Data]
Feb 24, 2022 - Bunz Group
Maier, Steffen; Heckershoff, Robin; Wurm, Thomas; Biegger, Philipp; Brödner, Kerstin; Krämer, Petra; Hoffmann, Marvin; Eberle, Lukas; Stein, Jana; Rominger, Frank; Rudolph, Matthias; Freudenberg, Jan; Dreuw, Andreas; Hashmi, Stephen; Bunz, Uwe, 2022, "Cyclopentannulated Dihydrotetraazapentacenes [Data]", https://doi.org/10.11588/data/PZGMSS, heiDATA, V1
The transition-metal catalyzed cyclization of bissilylethynylated N,N’-dihydro¬tetra¬aza¬pentacene (TIPS-TAP-H2) into bissilylated cyclo¬penta¬[fg,qr]¬pentacenes is reported. Depending on the catalyst either none, one or two silyl groups migrate and change their positions in the...
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