Institute of Organic Chemistry

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1 to 10 of 301 Results

VT NMR Experiments.zip Jan 17, 2022 - Soluble Congeners of Prior Insoluble Shape‐Persistent Imine Cages [Data] ZIP Archive - 16.6 MB - MD5: 81feeb5c93495f4cb6a5eda343c86df4
Two Dimensional Triptycene End-Capping and Its Influence on the Self-Assembly of Quinoxalinophenanthrophenazines [Data] Mar 27, 2023 Roß, Lisa; Reitemeier, Julius; Ghalami, Farhad; Zhang, Wen-Shan; Gross, Jürgen H.; Rominger, Frank; Elbert, Sven M.; Schröder, Rasmus; Elstner, Marcus; Mastalerz, Michael, 2023, "Two Dimensional Triptycene End-Capping and Its Influence on the Self-Assembly of Quinoxalinophenanthrophenazines [Data]", https://doi.org/10.11588/data/W3KWEJ, heiDATA, V1 A series of quinoxalinophenanthrophenazines (QPPs) with two-dimensional triptycene end-caps was synthesized from a triphenylene base ortho-diamine. UV/vis spectroscopy suggested the formation of dimers in solution which was further confirmed by MALDI-TIMS-TOF-MS and single crysta...
TableS4_SI_Time_Screening.zip Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data] ZIP Archive - 3.3 MB - MD5: d10bffee74494670f19fa9c28d5e9488
TableS3_SI_Concentration_Screening.zip Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data] ZIP Archive - 7.7 MB - MD5: d292cd5d60680ff7bdbc7499cdc1a6a4
TableS2_SI_Solvent_Screening.zip Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data] ZIP Archive - 58.6 MB - MD5: bcc2d367e132d489058b4c83de5d2a67
TableS1_SI_Stoichiometry_Screening.zip Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data] ZIP Archive - 13.4 MB - MD5: 4321a88dbceeff4368e4c725a3934122
Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data] Jan 24, 2022 Uhrmacher, Fabian; Elbert, Sven Michael; Rominger, Frank; Mastalerz, Michael, 2022, "Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]", https://doi.org/10.11588/data/LOR2JH, heiDATA, V1 Shape-persistent trinuclear Ni(II)- and Pt(II)-cage compounds with large cavities have been synthesized by using bissalicylaldehyde struts that contain the metal salphen units already. The Pt(II) derivative was investigated by single crystal X-ray diffraction.
Synthesis of Chiral Pyrene-Based 1,4-Dithiins [Data] Feb 22, 2024 Keck, Christoph; Rominger, Frank; Mastalerz, Michael, 2024, "Synthesis of Chiral Pyrene-Based 1,4-Dithiins [Data]", https://doi.org/10.11588/data/NCRUAV, heiDATA, V1 The 1,4-dithiin motif is known for its reversible redox properties to generate radical cations and diradical dications and thus is interesting for organic electronic applications. However, examples where this motif is embedded into chiral larger fused aromatic compounds is very r...
Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data] Aug 23, 2023 Kirschbaum, Tobias; Rominger, Frank; Mastalerz, Michael, 2023, "Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data]", https://doi.org/10.11588/data/JE8LF7, heiDATA, V1 A benzotrisazulene was synthesized on the basis of a truxene precursor by a series of Suzuki–Miyaura reactions via the intermediate trisoxo compound. The latter occurs in two forms (syn and anti), and the syn forms porous crystals.
Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data] Aug 23, 2023 Wagner, Philippe; Rominger, Frank; Gross, Jürgen H.; Mastalerz, Michael, 2023, "Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]", https://doi.org/10.11588/data/TIYBD2, heiDATA, V1 A quadruply interlocked catenane has been formed from giant chiral [8+12] salicylimine cubes in a reaction that can be controlled by the reaction solvent. Single-crystal X-ray diffraction revealed hydrogen bonding to be a central driving force for the catenation. Furthermore, scr...

VT NMR Experiments.zip

Jan 17, 2022 - Soluble Congeners of Prior Insoluble Shape‐Persistent Imine Cages [Data]

ZIP Archive - 16.6 MB -

Two Dimensional Triptycene End-Capping and Its Influence on the Self-Assembly of Quinoxalinophenanthrophenazines [Data]

Mar 27, 2023

Roß, Lisa; Reitemeier, Julius; Ghalami, Farhad; Zhang, Wen-Shan; Gross, Jürgen H.; Rominger, Frank; Elbert, Sven M.; Schröder, Rasmus; Elstner, Marcus; Mastalerz, Michael, 2023, "Two Dimensional Triptycene End-Capping and Its Influence on the Self-Assembly of Quinoxalinophenanthrophenazines [Data]", https://doi.org/10.11588/data/W3KWEJ, heiDATA, V1

A series of quinoxalinophenanthrophenazines (QPPs) with two-dimensional triptycene end-caps was synthesized from a triphenylene base ortho-diamine. UV/vis spectroscopy suggested the formation of dimers in solution which was further confirmed by MALDI-TIMS-TOF-MS and single crysta...

TableS4_SI_Time_Screening.zip

Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]

ZIP Archive - 3.3 MB -

TableS3_SI_Concentration_Screening.zip

Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]

ZIP Archive - 7.7 MB -

TableS2_SI_Solvent_Screening.zip

Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]

ZIP Archive - 58.6 MB -

TableS1_SI_Stoichiometry_Screening.zip

Aug 23, 2023 - Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]

ZIP Archive - 13.4 MB -

Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]

Jan 24, 2022

Uhrmacher, Fabian; Elbert, Sven Michael; Rominger, Frank; Mastalerz, Michael, 2022, "Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]", https://doi.org/10.11588/data/LOR2JH, heiDATA, V1

Shape-persistent trinuclear Ni(II)- and Pt(II)-cage compounds with large cavities have been synthesized by using bissalicylaldehyde struts that contain the metal salphen units already. The Pt(II) derivative was investigated by single crystal X-ray diffraction.

Synthesis of Chiral Pyrene-Based 1,4-Dithiins [Data]

Feb 22, 2024

Keck, Christoph; Rominger, Frank; Mastalerz, Michael, 2024, "Synthesis of Chiral Pyrene-Based 1,4-Dithiins [Data]", https://doi.org/10.11588/data/NCRUAV, heiDATA, V1

The 1,4-dithiin motif is known for its reversible redox properties to generate radical cations and diradical dications and thus is interesting for organic electronic applications. However, examples where this motif is embedded into chiral larger fused aromatic compounds is very r...

Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data]

Aug 23, 2023

Kirschbaum, Tobias; Rominger, Frank; Mastalerz, Michael, 2023, "Synthesis of a Benzotrisazulene via Trioxobenzotrisazulene [data]", https://doi.org/10.11588/data/JE8LF7, heiDATA, V1

A benzotrisazulene was synthesized on the basis of a truxene precursor by a series of Suzuki–Miyaura reactions via the intermediate trisoxo compound. The latter occurs in two forms (syn and anti), and the syn forms porous crystals.

Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]

Aug 23, 2023

Wagner, Philippe; Rominger, Frank; Gross, Jürgen H.; Mastalerz, Michael, 2023, "Solvent-Controlled Quadruple Catenation of Giant Chiral [8+12] Salicylimine Cubes Driven by Weak Hydrogen Bonding [Data]", https://doi.org/10.11588/data/TIYBD2, heiDATA, V1

A quadruply interlocked catenane has been formed from giant chiral [8+12] salicylimine cubes in a reaction that can be controlled by the reaction solvent. Single-crystal X-ray diffraction revealed hydrogen bonding to be a central driving force for the catenation. Furthermore, scr...

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