3D Matter Made to Order (3DMM2O)

Data publications from the Cluster of Excellence 3D Matter Made to Order (3DMM2O). The Cluster is a collaboration of Karlsruhe Institute of Technology (KIT) and Heidelberg University. It pursues an interdisciplinary approach through conjunction of natural, engineering, and social sciences. 3DMM2O establishes scalable digital 3D Additive Manufacturing transcending from the molecular to the macroscopic scale. The goal is the ultimate digitalization of 3D manufacturing and material processing.

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11 to 20 of 28 Results

Aqueous seeded RAFT polymerization for the preparation of self-assemblies containing nucleobase analogues [data] Feb 1, 2023 - Blasco Group Miriam Abad; Martina Nardi; Luis Oriol; Milagros Piñol; Eva Blasco, 2023, "Aqueous seeded RAFT polymerization for the preparation of self-assemblies containing nucleobase analogues [data]", https://doi.org/10.11588/data/U1O0NB, heiDATA, V1 Self-assemblies containing the nucleobase analogue 2,6-diacylaminopyridine (DAP) have been successfully prepared for the first time by aqueous seeded RAFT polymerization in high concentrations. For this purpose, a diblock copolymer containing poly(ethylene glycol) (PEG) and DAP p...
Late-Stage Functionalisation of Peptides on the Solid Phase by an Iodination-Substitution Approach [Research Data] Dec 19, 2022 - Thomas Lab Werner, Marius; Pampel, Julius; Pham, Truc Lam; Thomas, Franziska, 2022, "Late-Stage Functionalisation of Peptides on the Solid Phase by an Iodination-Substitution Approach [Research Data]", https://doi.org/10.11588/data/RG2NHY, heiDATA, V1 The functionalisation of peptides at a late synthesis stage holds great potential, for example, for the synthesis of peptide pharmaceuticals, fluorescent biosensors or peptidomimetics. Here we describe an on-resin iodination-substitution reaction sequence on homoserine that is al...
A Facile Approach for 4D Microprinting of Multi-Photoresponsive Actuators [data] Nov 2, 2022 - Blasco Group Hsu, Li-Yun; Mainik, Philipp; Münchinger, Alexander; Lindenthal, Sebastian; Spratte, Tobias; Welle, Alexander; Zaumseil, Jana; Selhuber-Unkel, Christine; Wegener, Martin; Blasco, Eva, 2022, "A Facile Approach for 4D Microprinting of Multi-Photoresponsive Actuators [data]", https://doi.org/10.11588/data/MR5H4A, heiDATA, V1 For microscale 4D photoresponsive actuators, light is crucial in two ways. First, the underlying additive manufacturing techniques rely on photopolymerization processes triggered by the absorption of light. Second, the absorption of light serves as the actuation stimulus. The two...
Electron-beam lithography of cinnamate polythiophene films: conductive nanorods for electronic applications [Data] Jul 5, 2022 - Bunz Group Bojanowski, N. Maximilian; Huck, Christian; Veith, Lisa; Strunk, Karl-Philipp; Bäuerle, Rainer; Melzer, Christian; Freudenberg, Jan; Wacker, Irene; Schröder, Rasmus R.; Tegeder, Petra; Bunz, Uwe H. F., 2022, "Electron-beam lithography of cinnamate polythiophene films: conductive nanorods for electronic applications [Data]", https://doi.org/10.11588/data/ZJAT9A, heiDATA, V1 Research Data associated with the related publication. Synthesis and characterization of cinnamate substituted polythiophene (P3ZT). Cross linkage via UV and electron beam radiation; network formation in thin films controlled by infrared spectroscopy and film retention experiment...
The CSY-protecting group in the microwave-assisted synthesis of aggregation-prone peptides [Research Data] Mar 24, 2022 - Thomas Lab Pham, Truc Lam; Zilke, Jennifer; Müller, Christine Charlotte; Thomas, Franziska, 2022, "The CSY-protecting group in the microwave-assisted synthesis of aggregation-prone peptides [Research Data]", https://doi.org/10.11588/data/ECKCUY, heiDATA, V1 This report describes the application of cyanosulfurylide (CSY)-protected aspartatic acid building blocks in microwave-assisted synthesis of aggregation-prone protein domains. We present a synthesis of Fmoc-Asp(CSY)-OH on a multigram scale, as well as procedures for the microwave...
Printing and Erasing of DNA-based Photoresists inside Synthetic Cells [RESEARCH DATA] Feb 28, 2022 - Göpfrich Group - Biophysical Engineering of Life Goepfrich, Kerstin; Walther, Tobias, 2022, "Printing and Erasing of DNA-based Photoresists inside Synthetic Cells [RESEARCH DATA]", https://doi.org/10.11588/data/MKOC9S, heiDATA, V1 In the pursuit to produce functioning synthetic cells from the bottom up, DNA nanotechnology has proven to be a powerful tool. However, the crowded yet highly organized arrangement in living cells, bridging from the nano- to the micron-scale, remains challenging to recreate with...
Desymmetrization Strategy to Achieve Triptycene-Based 3,6-Dimethoxytriphenylenes via Oxidative Cyclodehydrogenation [Data] Feb 4, 2022 - Institute of Organic Chemistry - AK Mastalerz Reinhard, Dennis; Rominger, Frank; Mastalerz, Michael, 2022, "Desymmetrization Strategy to Achieve Triptycene-Based 3,6-Dimethoxytriphenylenes via Oxidative Cyclodehydrogenation [Data]", https://doi.org/10.11588/data/OH6757, heiDATA, V1 To achieve a highly symmetric triptycene based hexamethoxytriphenylene in high yield of 97 %, a less symmetric triptycene (C3v) is necessary as precursor for cyclodehydrogenative Scholl-type oxidation, by taking into account the regioselectivity of the C-C bond formation controll...
Visualizing morphological principles for efficient photocurrent generation in organic non-fullerene acceptor blends [Research data] Jan 24, 2022 - CryoEM Köntges, Wolfgang; Perkhun, Pavlo; Kammerer, Jochen; Alkarsifi, Riva; Würfel, Uli; Margeat, Olivier; Videlot-Ackermann, Christine; Simon, Jean-Jacques; Schröder, Rasmus R.; Ackermann, Jörg; Pfannmöller, Martin, 2022, "Visualizing morphological principles for efficient photocurrent generation in organic non-fullerene acceptor blends [Research data]", https://doi.org/10.11588/data/ZW8JL9, heiDATA, V1 Research Data associated with the related publication.
Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data] Jan 24, 2022 - Institute of Organic Chemistry - AK Mastalerz Uhrmacher, Fabian; Elbert, Sven Michael; Rominger, Frank; Mastalerz, Michael, 2022, "Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]", https://doi.org/10.11588/data/LOR2JH, heiDATA, V1 Shape-persistent trinuclear Ni(II)- and Pt(II)-cage compounds with large cavities have been synthesized by using bissalicylaldehyde struts that contain the metal salphen units already. The Pt(II) derivative was investigated by single crystal X-ray diffraction.
Switchable Zinc (II)-Responsive Globular β-Sheet Peptide [Research Data] Jan 19, 2022 - Thomas Lab Pham, Truc Lam; Kovermann, Michael; Thomas, Franziska, 2022, "Switchable Zinc (II)-Responsive Globular β-Sheet Peptide [Research Data]", https://doi.org/10.11588/data/HV4MJW, heiDATA, V1 The natural function of many proteins depends on their ability to switch their conformation driven by environmental changes. In this work, we present a small, monomeric β-sheet peptide that switches between a molten globule and a folded state through Zn(II) binding. The solvent-e...

Aqueous seeded RAFT polymerization for the preparation of self-assemblies containing nucleobase analogues [data]

Feb 1, 2023 - Blasco Group

Miriam Abad; Martina Nardi; Luis Oriol; Milagros Piñol; Eva Blasco, 2023, "Aqueous seeded RAFT polymerization for the preparation of self-assemblies containing nucleobase analogues [data]", https://doi.org/10.11588/data/U1O0NB, heiDATA, V1

Self-assemblies containing the nucleobase analogue 2,6-diacylaminopyridine (DAP) have been successfully prepared for the first time by aqueous seeded RAFT polymerization in high concentrations. For this purpose, a diblock copolymer containing poly(ethylene glycol) (PEG) and DAP p...

Late-Stage Functionalisation of Peptides on the Solid Phase by an Iodination-Substitution Approach [Research Data]

Dec 19, 2022 - Thomas Lab

Werner, Marius; Pampel, Julius; Pham, Truc Lam; Thomas, Franziska, 2022, "Late-Stage Functionalisation of Peptides on the Solid Phase by an Iodination-Substitution Approach [Research Data]", https://doi.org/10.11588/data/RG2NHY, heiDATA, V1

The functionalisation of peptides at a late synthesis stage holds great potential, for example, for the synthesis of peptide pharmaceuticals, fluorescent biosensors or peptidomimetics. Here we describe an on-resin iodination-substitution reaction sequence on homoserine that is al...

A Facile Approach for 4D Microprinting of Multi-Photoresponsive Actuators [data]

Nov 2, 2022 - Blasco Group

Hsu, Li-Yun; Mainik, Philipp; Münchinger, Alexander; Lindenthal, Sebastian; Spratte, Tobias; Welle, Alexander; Zaumseil, Jana; Selhuber-Unkel, Christine; Wegener, Martin; Blasco, Eva, 2022, "A Facile Approach for 4D Microprinting of Multi-Photoresponsive Actuators [data]", https://doi.org/10.11588/data/MR5H4A, heiDATA, V1

For microscale 4D photoresponsive actuators, light is crucial in two ways. First, the underlying additive manufacturing techniques rely on photopolymerization processes triggered by the absorption of light. Second, the absorption of light serves as the actuation stimulus. The two...

Electron-beam lithography of cinnamate polythiophene films: conductive nanorods for electronic applications [Data]

Jul 5, 2022 - Bunz Group

Bojanowski, N. Maximilian; Huck, Christian; Veith, Lisa; Strunk, Karl-Philipp; Bäuerle, Rainer; Melzer, Christian; Freudenberg, Jan; Wacker, Irene; Schröder, Rasmus R.; Tegeder, Petra; Bunz, Uwe H. F., 2022, "Electron-beam lithography of cinnamate polythiophene films: conductive nanorods for electronic applications [Data]", https://doi.org/10.11588/data/ZJAT9A, heiDATA, V1

Research Data associated with the related publication. Synthesis and characterization of cinnamate substituted polythiophene (P3ZT). Cross linkage via UV and electron beam radiation; network formation in thin films controlled by infrared spectroscopy and film retention experiment...

The CSY-protecting group in the microwave-assisted synthesis of aggregation-prone peptides [Research Data]

Mar 24, 2022 - Thomas Lab

Pham, Truc Lam; Zilke, Jennifer; Müller, Christine Charlotte; Thomas, Franziska, 2022, "The CSY-protecting group in the microwave-assisted synthesis of aggregation-prone peptides [Research Data]", https://doi.org/10.11588/data/ECKCUY, heiDATA, V1

This report describes the application of cyanosulfurylide (CSY)-protected aspartatic acid building blocks in microwave-assisted synthesis of aggregation-prone protein domains. We present a synthesis of Fmoc-Asp(CSY)-OH on a multigram scale, as well as procedures for the microwave...

Printing and Erasing of DNA-based Photoresists inside Synthetic Cells [RESEARCH DATA]

Feb 28, 2022 - Göpfrich Group - Biophysical Engineering of Life

Goepfrich, Kerstin; Walther, Tobias, 2022, "Printing and Erasing of DNA-based Photoresists inside Synthetic Cells [RESEARCH DATA]", https://doi.org/10.11588/data/MKOC9S, heiDATA, V1

In the pursuit to produce functioning synthetic cells from the bottom up, DNA nanotechnology has proven to be a powerful tool. However, the crowded yet highly organized arrangement in living cells, bridging from the nano- to the micron-scale, remains challenging to recreate with...

Desymmetrization Strategy to Achieve Triptycene-Based 3,6-Dimethoxytriphenylenes via Oxidative Cyclodehydrogenation [Data]

Feb 4, 2022 - Institute of Organic Chemistry - AK Mastalerz

Reinhard, Dennis; Rominger, Frank; Mastalerz, Michael, 2022, "Desymmetrization Strategy to Achieve Triptycene-Based 3,6-Dimethoxytriphenylenes via Oxidative Cyclodehydrogenation [Data]", https://doi.org/10.11588/data/OH6757, heiDATA, V1

To achieve a highly symmetric triptycene based hexamethoxytriphenylene in high yield of 97 %, a less symmetric triptycene (C3v) is necessary as precursor for cyclodehydrogenative Scholl-type oxidation, by taking into account the regioselectivity of the C-C bond formation controll...

Visualizing morphological principles for efficient photocurrent generation in organic non-fullerene acceptor blends [Research data]

Jan 24, 2022 - CryoEM

Köntges, Wolfgang; Perkhun, Pavlo; Kammerer, Jochen; Alkarsifi, Riva; Würfel, Uli; Margeat, Olivier; Videlot-Ackermann, Christine; Simon, Jean-Jacques; Schröder, Rasmus R.; Ackermann, Jörg; Pfannmöller, Martin, 2022, "Visualizing morphological principles for efficient photocurrent generation in organic non-fullerene acceptor blends [Research data]", https://doi.org/10.11588/data/ZW8JL9, heiDATA, V1

Research Data associated with the related publication.

Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]

Jan 24, 2022 - Institute of Organic Chemistry - AK Mastalerz

Uhrmacher, Fabian; Elbert, Sven Michael; Rominger, Frank; Mastalerz, Michael, 2022, "Synthesis of Large [2+3] Salicylimine Cages with Embedded Metal-Salphen Units [Data]", https://doi.org/10.11588/data/LOR2JH, heiDATA, V1

Shape-persistent trinuclear Ni(II)- and Pt(II)-cage compounds with large cavities have been synthesized by using bissalicylaldehyde struts that contain the metal salphen units already. The Pt(II) derivative was investigated by single crystal X-ray diffraction.

Switchable Zinc (II)-Responsive Globular β-Sheet Peptide [Research Data]

Jan 19, 2022 - Thomas Lab

Pham, Truc Lam; Kovermann, Michael; Thomas, Franziska, 2022, "Switchable Zinc (II)-Responsive Globular β-Sheet Peptide [Research Data]", https://doi.org/10.11588/data/HV4MJW, heiDATA, V1

The natural function of many proteins depends on their ability to switch their conformation driven by environmental changes. In this work, we present a small, monomeric β-sheet peptide that switches between a molten globule and a folded state through Zn(II) binding. The solvent-e...

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