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Part 1: Document Description
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Citation |
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Title: |
Deconstructing 3D Structured Materials by Modern Ultramicrotomy for Multimodal Imaging and Volume Analysis Across Length Scales [Research data and source code] |
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Identification Number: |
doi:10.11588/data/TOEQZB |
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Distributor: |
heiDATA |
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Date of Distribution: |
2023-07-11 |
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Version: |
1 |
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Bibliographic Citation: |
Wacker, Irene; Curticean, Ronald; Ryklin, Daniel; Weidinger, Britta; Mayer, Frederik; Huang, Li-Yu; Hoffmann, Julian; Islam, Monsur; von Coelln, Nadine; Schmitt, Tanja; Huck, Christian; Tegeder, Petra; Feist, Florian; Kammerer, Jochen A.; Barner-Kowollik, Christopher; Wegener, Martin; Blasco, Eva; Gengenbach, Ulrich; Schröder, Rasmus R., 2023, "Deconstructing 3D Structured Materials by Modern Ultramicrotomy for Multimodal Imaging and Volume Analysis Across Length Scales [Research data and source code]", https://doi.org/10.11588/data/TOEQZB, heiDATA, V1 |
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Citation |
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Title: |
Deconstructing 3D Structured Materials by Modern Ultramicrotomy for Multimodal Imaging and Volume Analysis Across Length Scales [Research data and source code] |
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Identification Number: |
doi:10.11588/data/TOEQZB |
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Authoring Entity: |
Wacker, Irene (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Heidelberg University Hospital, BioQuant, Cryo Electron Microscopy) |
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Curticean, Ronald (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Heidelberg University Hospital, BioQuant, Cryo Electron Microscopy) |
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Ryklin, Daniel (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Heidelberg University Hospital, BioQuant, Cryo Electron Microscopy) |
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Weidinger, Britta (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and IMSEAM, Universität Heidelberg) |
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Mayer, Frederik (KIT, Cluster of Excellence "3DMM2O"; KIT and Institute of Nanotechnology (INT), Karlsruhe Institute of Technology (KIT)) |
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Huang, Li-Yu (Institute for Automation and Applied Informatics, Karlsruhe Institute of Technology (KIT)) |
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Hoffmann, Julian (Institute for Automation and Applied Informatics, Karlsruhe Institute of Technology (KIT)) |
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Islam, Monsur (KIT, Cluster of Excellence "3DMM2O"; KIT and Institute of Microstructure Technology (IMT) Karlsruhe Institute of Technology (KIT)) |
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von Coelln, Nadine (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Physikalisch-Chemisches Institut, Universität Heidelberg) |
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Schmitt, Tanja (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Physikalisch-Chemisches Institut, Universität Heidelberg) |
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Huck, Christian (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Physikalisch-Chemisches Institut, Universität Heidelberg) |
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Tegeder, Petra (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Physikalisch-Chemisches Institut, Universität Heidelberg) |
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Feist, Florian (KIT, Cluster of Excellence "3DMM2O"; KIT and Institute of Nanotechnology (INT), Karlsruhe Institute of Technology (KIT)) |
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Kammerer, Jochen A. (School of Chemistry and Physics, Centre for Materials Science, Queensland University of Technology (QUT)) |
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Barner-Kowollik, Christopher (School of Chemistry and Physics, Centre for Materials Science, Queensland University of Technology (QUT)) |
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Wegener, Martin (KIT, Cluster of Excellence "3DMM2O"; KIT and Institute of Nanotechnology (INT), Karlsruhe Institute of Technology (KIT)) |
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Blasco, Eva (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and IMSEAM, Universität Heidelberg) |
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Gengenbach, Ulrich (Institute for Automation and Applied Informatics, Karlsruhe Institute of Technology (KIT)) |
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Schröder, Rasmus R. (Heidelberg University, Cluster of Excellence "3DMM2O"; Heidelberg University and Heidelberg University Hospital, BioQuant, Cryo Electron Microscopy) |
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Distributor: |
heiDATA |
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Access Authority: |
Wacker, Irene |
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Access Authority: |
Schröder, Rasmus R. |
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Holdings Information: |
https://doi.org/10.11588/data/TOEQZB |
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Study Scope |
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Keywords: |
Chemistry, Other, structured materials, 3D microscopy, ultramicrotomy, array tomography, CLEM, probe microscopy, spectroscopy |
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Abstract: |
Based on the rapid advances in additive manufacturing, micro-patterned heterostructures of soft materials have become available that need to be characterized down to the nanoscale. Advanced function-structure relationships are designed by direct 3D structuring of the object and – in the future – fine control over material functionality in 3D will produce complex functional objects. To control their design, fabrication and final structure, morphological and spectroscopical imaging in 3D at nanometer resolution are critically required. With examples of carbon-based objects, it is demonstrated how serial ultramicrotomy, that is, cutting a large number of successive ultrathin sections, can be utilized to gain access to the interior of 3D objects. Array tomography, hierarchical imaging and correlative light and electron microscopy can bridge length scales over several orders of magnitude and provide multimodal information of the sample's inner structure. Morphology data derived from scanning electron microscopy are correlated with spectroscopy in analytical transmission electron microscopy and probe microscopy at nanometer resolution, using TEM-electron energy loss spectroscopy and infrared-scanning-near-field microscopy. The correlation of different imaging modalities and spectroscopy of carbon-based materials in 3D provides a powerful toolbox of complementary techniques for understanding emerging functions from nanoscopic structuring. |
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Methodology and Processing |
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Sources Statement |
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Data Access |
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Other Study Description Materials |
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Related Publications |
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Citation |
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Title: |
Wacker, Irene; Curticean, Ronald; Ryklin, Daniel; Weidinger, Britta; Mayer, Frederik; Huang, Li-Yu; Hoffmann, Julian; Islam, Monsur; von Coelln, Nadine; Schmitt, Tanja; Huck, Christian; Tegeder, Petra; Feist, Florian; Kammerer, Jochen A.; Barner-Kowollik, Christopher; Wegener, Martin; Blasco, Eva; Gengenbach, Ulrich; Schröder, Rasmus R., 2023, "Deconstructing 3D Structured Materials by Modern Ultramicrotomy for Multimodal Imaging and Volume Analysis Across Length Scales". Advanced Functional Materials (2023). |
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Identification Number: |
10.1002/adfm.202302025 |
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Bibliographic Citation: |
Wacker, Irene; Curticean, Ronald; Ryklin, Daniel; Weidinger, Britta; Mayer, Frederik; Huang, Li-Yu; Hoffmann, Julian; Islam, Monsur; von Coelln, Nadine; Schmitt, Tanja; Huck, Christian; Tegeder, Petra; Feist, Florian; Kammerer, Jochen A.; Barner-Kowollik, Christopher; Wegener, Martin; Blasco, Eva; Gengenbach, Ulrich; Schröder, Rasmus R., 2023, "Deconstructing 3D Structured Materials by Modern Ultramicrotomy for Multimodal Imaging and Volume Analysis Across Length Scales". Advanced Functional Materials (2023). |
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Label: |
00_ReadMe_20230708.txt |
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Notes: |
text/plain |
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Label: |
Block Copolymer Data.zip |
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Notes: |
application/zip |
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Label: |
EELS Data Processing.zip |
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Notes: |
application/zip |
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Label: |
Graphitized Origami Data.zip |
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Notes: |
application/zip |
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Label: |
Porosity.zip |
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Notes: |
application/zip |
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Label: |
SNOM Data.zip |
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Notes: |
application/zip |